180
e
H
E
M
Sill I!'I/I,¡,r:iuc duo"'po/l"•
.'d
bJ n,id,.
INT o
~ I~rgc
IlIbulalcd reton 1'"1 a fmal l
qu~nti ly
of
fal alOmoni.,e in powder: fel
~'our
,ctCln in a fu nll':"
and IlIle 00"
I~rgc
ballon,
~s
in Ihe cli ll<II.llio', of Ih,' f,,:.,–
king aeids of nilre and f'ca- fJIL T hrough ,he I",le in
your relon pour a quantity of nil of \'¡Iriol or f"irit
of niue equal in wcight to your (;113ml11<11,i.,e. An ef
fervefecnce \\'ill inOaod
y
follow. T he
mlxlur~
\\'ill f\Vd l,
and d.fcharge while vapours ·vhieh will come Ol'e( into
lhe reeeiv'r. SIOP thc whole in Ihe reton illlmcdialely ,
and let the fi rll vapou rs pafs over, togt'lhtr widl IlImc
drops of liquor, \Vhieh will diOil Wilholll 6re. T hen
pUl
~
few eoals' imo Ihe fll roaee, and eonlinue Ihe diOil–
lalion Wi lh a very gende heat ; whieh however muObe
inemfed lilde bylinle lill nOlhing more will e"me over
When Ihe operalion is fimOled. you will find io Ihe ,e–
(eiver a fpiril of fa\¡ if
)'011
made ufe of oil 01' vilri.:1 or
an
aq/la "gil,
if Ihe fpiril or nilre was emplo)'ed: aod
in the reton will he lefl a f.line mafs, whieh will ,le ei·
ther a glauber's feercI r.d ammoniae, or a nilrOIlS r.,1
ammoniae, aeeording 10 ,he nal'lrc of Ihe aeid ufed tO
deeompound Ihe fal ammuniae.
SQ/ alll/llol/inc drcompoundfd
by
fiud .mali,.
V.la–lile foil.
'!he
Ftbrif/lge
o/
S),lvitu.
lNTo a glafs alembic or retort put fa l ammoniac and
fall of lartar pulverife,] and mixed togt'lher in
tqu~1
quanlllies. Sel your velfe! in.a proper
~U\'naee, ~~d i~medialely IUle on a luge rew ver. A hule vol.,ule fp'–
rit will afeend; aod a I'olalile alkali, in aeonerele form,
very while and beautiful will fublinlt inlo the head, and
come over into Ihe reeeiver, in quaotity
ne.IrtwO Ihi rds
or dmefounhs of the fal ammooiae ufed . ContiOl'e the
diOollation. inere, fing Ihe fire byJegret still nothiog mOre
will fnblime. Then unlute lhe
\'~lfels.
Put up your
•0lHile fa lt immediatelyinto a wide mouthed bonle and
llop it elote with a cryllal flopple. At the botlom of
the retort or eucurbit )'OUwill fiod a falin: mafs, which,
being dilfolved and cryOallifed, will for m a falt oearly
cubie~1.
hal'iog the taOe and otha propenies of
f~a-f.h .
T his is Ihe
fal f,bri(ug /l l/l jifvii.
Sal Ammoniac
d(col/lp',un~ed
hJ ahjorhenl Earlh, and
Lil/le.
F,ud S"I AI/IIIIOnidc.
Ln
one pan of fal ammoniac and Ihree pans of lime
s
T
II
Y.
n:lk~d
in Ihe air be pu"elir«1repal'atdy, aod expedili–
(lI,l1y mi..,,1
1O.~e
!ler.
PUl Ihi3 '.II xturt
1I1l1II,dwdy
intu a g!.,fs rClOft, fo IHrge Ihat 1,,11
lIt
,t nmy relllollll
emply
JI
pply Ihcreto a capaelOus
rtC<lV~I',
W'lll
d
f.1I.III hol . ill ,t to gil'e
v~nt
to Ihc vapours , if
ne~u."1.
L,·: your retor! nan" io lhe furn,ce .,bou t a 'Iualler 01'
an h,,"r, I'."tl:ollt any li re under
11 .
\Vlllle it 1I.,ods thu1,
a g;cat qu.IIlIily of invi!;!'le \·.'follrs " id ,;Ic, eor.uen:c
ioto drQPs, aaJ form
li~nol'
io lhe rceell er. Tl,en pUl
two or lh"c live
eo.lsio yuur fUl l1aee, alld gladu,lIy
ine, e.f~
lhe fi,e ti ll 00 more li'lnnr will rife. Now UII–
I"te your
vcn~ls. tak,n~
.111 p"lIible eare
10
avoid the Va–
ponrs, and quiekly pour thc liqllor out o the rece,.er
ioto a boule, wh,ch )'on mnfi /lop IVith a
cryn~l lt"pple,
rubbed wilh emcry. There \Vi II ,cmilin. at Ihe botltlm
01 the retort, a \Vhite mafs, coofilboll of the "me elll–
plo)ed in Ihe diOill. liun, logelhn W,t
th~
a, iJ of the
f.1amlDoniac: this is ealled
fi.rdl al al//1IIMiac.
Volali/e Alioli, L'CIIII,inrd .vill, .i9' lI.'al/m .
d
V..
lalile Oil;' Ar.'l/nlic
¡'/I.
Pl'
LVE P. ' SE
ard mix togethrr cqual
plns
of fal am–
moniac ilnJ fJh of tartar : put the OIi>:lure ioto a glafl
or /looe elleurbit: pour on it gQod fp"it
~f.
wioe tllI il'
rif~
h.M an inch aboye the mane r. Mix the whule ",idl
a wood"n
fpatul~;
apply
:1
head ,nd a ,eceiver, and di–
Uil in a faod -balh, gently hemd, for
t \Vo
or thrce hours.
A volatile fa lt \ViII "fe ioto lhe head; and lhen the rpirit
of \Vine \ViII dill.1
lOto
the recr,ver, earryiog with it a
pon ion of the v"lalile
f.dt.
When oothing more will come orer, lel your
n(f.!5
cool ; then unlute them, fcparm the volallle fan, dud
weigh it dil'ctlly. Returo it into
~
glafs eucurbit, an,1
for
ever~
ollnee thereof adJ a tlr.m aotl a hall
01
elrrn–
tial o", dra·.vn froln one or more fom of uomatic
pl, nts. Slir the \VIde IVllh a wcoJen fpanl!.l , that the
clfen:e
m~y
iocorpnrate
thorou~hly
wll h the volatile
111r.
Coyer the eueurbit ",ilh a head, ht
00
a receiver,
~nd ,
h.lving lutcd it e, a{\ly, dillil in a fand-balh, as befl'ff,
with a ve,y gen le hcat. AII the volatile rah will "le,
and Oiek 10 the
hc~d .
Let the (¡,e go OUt,
ano
"hca
the velfels are cooled take )Ollr falt Out 01' the
hc~d,
It
IVill have an odour eompouoded or in OIVO
prup~r
fm:!I, and Ihe fmell of Ihe elfeoee with whieh it is CIIm–
!ti, cd This is an
nf9ll/tllic
ú&·
lull .
PUl it iOlo a
boltl~
flopped clofe wiln a cryllJI nopple.
A T AB Lr ...