Table of Contents Table of Contents
Previous Page  212 / 1042 Next Page
Information
Show Menu
Previous Page 212 / 1042 Next Page
Page Background

180

e

H

E

M

Sill I!'I/I,¡,r:iuc duo"'po/l"•

.'d

bJ n,id,.

INT o

~ I~rgc

IlIbulalcd reton 1'"1 a fmal l

qu~nti ly

of

fal alOmoni.,e in powder: fel

~'our

,ctCln in a fu nll':"

and IlIle 00"

I~rgc

ballon,

~s

in Ihe cli ll<II.llio', of Ih,' f,,:.,–

king aeids of nilre and f'ca- fJIL T hrough ,he I",le in

your relon pour a quantity of nil of \'¡Iriol or f"irit

of niue equal in wcight to your (;113ml11<11,i.,e. An ef

fervefecnce \\'ill inOaod

y

follow. T he

mlxlur~

\\'ill f\Vd l,

and d.fcharge while vapours ·vhieh will come Ol'e( into

lhe reeeiv'r. SIOP thc whole in Ihe reton illlmcdialely ,

and let the fi rll vapou rs pafs over, togt'lhtr widl IlImc

drops of liquor, \Vhieh will diOil Wilholll 6re. T hen

pUl

~

few eoals' imo Ihe fll roaee, and eonlinue Ihe diOil–

lalion Wi lh a very gende heat ; whieh however muObe

inemfed lilde bylinle lill nOlhing more will e"me over

When Ihe operalion is fimOled. you will find io Ihe ,e–

(eiver a fpiril of fa\¡ if

)'011

made ufe of oil 01' vilri.:1 or

an

aq/la "gil,

if Ihe fpiril or nilre was emplo)'ed: aod

in the reton will he lefl a f.line mafs, whieh will ,le ei·

ther a glauber's feercI r.d ammoniae, or a nilrOIlS r.,1

ammoniae, aeeording 10 ,he nal'lrc of Ihe aeid ufed tO

deeompound Ihe fal ammuniae.

SQ/ alll/llol/inc drcompoundfd

by

fiud .mali,.

V.la–

lile foil.

'!he

Ftbrif/lge

o/

S),lvitu.

lNTo a glafs alembic or retort put fa l ammoniac and

fall of lartar pulverife,] and mixed togt'lher in

tqu~1

quanlllies. Sel your velfe! in.a proper

~U\'naee, ~~d i~medialely IUle on a luge rew ver. A hule vol.,ule fp'–

rit will afeend; aod a I'olalile alkali, in aeonerele form,

very while and beautiful will fublinlt inlo the head, and

come over into Ihe reeeiver, in quaotity

ne.Ir

twO Ihi rds

or dmefounhs of the fal ammooiae ufed . ContiOl'e the

diOollation. inere, fing Ihe fire byJegret still nothiog mOre

will fnblime. Then unlute lhe

\'~lfels.

Put up your

•0lHile fa lt immediatelyinto a wide mouthed bonle and

llop it elote with a cryllal flopple. At the botlom of

the retort or eucurbit )'OUwill fiod a falin: mafs, which,

being dilfolved and cryOallifed, will for m a falt oearly

cubie~1.

hal'iog the taOe and otha propenies of

f~a-f.h .

T his is Ihe

fal f,bri(ug /l l/l jifvii.

Sal Ammoniac

d(col/lp',un~ed

hJ ahjorhenl Earlh, and

Lil/le.

F,ud S"I AI/IIIIOnidc.

Ln

one pan of fal ammoniac and Ihree pans of lime

s

T

II

Y.

n:lk~d

in Ihe air be pu"elir«1repal'atdy, aod expedili–

(lI,l1y mi..,,1

1O.~e

!ler.

PUl Ihi3 '.II xturt

1I1l1II,dwdy

intu a g!.,fs rClOft, fo IHrge Ihat 1,,11

lIt

,t nmy relllollll

emply

JI

pply Ihcreto a capaelOus

rtC<lV~I',

W'lll

d

f.1I.III hol . ill ,t to gil'e

v~nt

to Ihc vapours , if

ne~u."1.

L,·: your retor! nan" io lhe furn,ce .,bou t a 'Iualler 01'

an h,,"r, I'."tl:ollt any li re under

11 .

\Vlllle it 1I.,ods thu1,

a g;cat qu.IIlIily of invi!;!'le \·.'follrs " id ,;Ic, eor.uen:c

ioto drQPs, aaJ form

li~nol'

io lhe rceell er. Tl,en pUl

two or lh"c live

eo.ls

io yuur fUl l1aee, alld gladu,lIy

ine, e.f~

lhe fi,e ti ll 00 more li'lnnr will rife. Now UII–

I"te your

vcn~ls. tak,n~

.111 p"lIible eare

10

avoid the Va–

ponrs, and quiekly pour thc liqllor out o the rece,.er

ioto a boule, wh,ch )'on mnfi /lop IVith a

cryn~l lt"pple,

rubbed wilh emcry. There \Vi II ,cmilin. at Ihe botltlm

01 the retort, a \Vhite mafs, coofilboll of the "me elll–

plo)ed in Ihe diOill. liun, logelhn W,t

th~

a, iJ of the

f.1amlDoniac: this is ealled

fi.rd

l al al//1IIMiac.

Volali/e Alioli, L'CIIII,inrd .vill, .i9' lI.'al/m .

d

V..

lalile Oil;' Ar.'l/nlic

¡'/I.

Pl'

LVE P. ' SE

ard mix togethrr cqual

plns

of fal am–

moniac ilnJ fJh of tartar : put the OIi>:lure ioto a glafl

or /looe elleurbit: pour on it gQod fp"it

~f.

wioe tllI il'

rif~

h.M an inch aboye the mane r. Mix the whule ",idl

a wood"n

fpatul~;

apply

:1

head ,nd a ,eceiver, and di–

Uil in a faod -balh, gently hemd, for

t \Vo

or thrce hours.

A volatile fa lt \ViII "fe ioto lhe head; and lhen the rpirit

of \Vine \ViII dill.1

lOto

the recr,ver, earryiog with it a

pon ion of the v"lalile

f.dt

.

When oothing more will come orer, lel your

n(f.!5

cool ; then unlute them, fcparm the volallle fan, dud

weigh it dil'ctlly. Returo it into

~

glafs eucurbit, an,1

for

ever~

ollnee thereof adJ a tlr.m aotl a hall

01

elrrn–

tial o", dra·.vn froln one or more fom of uomatic

pl, nts. Slir the \VIde IVllh a wcoJen fpanl!.l , that the

clfen:e

m~y

iocorpnrate

thorou~hly

wll h the volatile

111r.

Coyer the eueurbit ",ilh a head, ht

00

a receiver,

~nd ,

h.lving lutcd it e, a{\ly, dillil in a fand-balh, as befl'ff,

with a ve,y gen le hcat. AII the volatile rah will "le,

and Oiek 10 the

hc~d .

Let the (¡,e go OUt,

ano

"hca

the velfels are cooled take )Ollr falt Out 01' the

hc~d,

It

IVill have an odour eompouoded or in OIVO

prup~r

fm:!I, and Ihe fmell of Ihe elfeoee with whieh it is CIIm–

!ti, cd This is an

nf9ll/tllic

ú&·

lull .

PUl it iOlo a

boltl~

flopped clofe wiln a cryllJI nopple.

A T AB Lr ...