e
JI
E
ni!hed, yon will find in Ihe rceeivcr a reflified dTential
oil, which will be clearer, thinner, .nd b<lIer feenurl
than befole it w,s Ihu! hl'lore re·dillillcd ; and in the
bOllomof the cucurbil will be lerl a malter of a deeprr
colour, more tcnacious, more refi nous, and of a
Icfs
grateful Imell.
Effential oil!, even Ihe purell, the bell prepared , and
lhe thinnel!,
foff,~r
greal
chan~es,
and are much impair.
td by growing old : Ihey gradn.llly lurn thiek and refino
ous; their f",eet, grmful feent is 1011, .nd fucceeded by
a more difagreeable fmell, fomewhat like Ihat or torpen·
lineo
The caufe of thefe ehanges is, that their finefl and
moll vol"ile part, that whirh eontains mol! of the odor·
ous principie, is diflipatcd and feparated fro.mthal whieb
conuins leall of il; which Iherefore grows thicker, and
comes fo mueb the nearer 10 the nalure of a refio, as Ihe
quantilY of acid, Ihal was dil!ribuled throllgh Ihe whole
oil befo re Ihe ditTipation of lhe more volalile pan, is, af·
ler fueh dilEpation, united and cooceotrated in the hea–
,'iefl parl; Ihe acid io oils being much leCs volalile than
lbe
odoro~s
pan, to which . Iooe they owe Illeir Icvity.
Heoce il appears whal preeautions are to be ured for
preferviog effer-tial oils as long as poflible without fpoil–
iog. They mufl be kept in a bOllle perfeétly wdl
1I0r'
pedo and always in a cool place, becaufe he"l quickly
diflipales thevolatile pam. Sorne authors direét thebOl–
tle tO be
k~pt
uoder water.
7. fire Oi/¡ by c07llbining Ihem 'WiJh highly cDnccn/raltd
AcidJ : ilijlanccd in Oil o/ 'Turlenline.
M
I
X
togelher in a glafs equal parts of coneentrated
oil of vitriol, aod highly Cmoking fre!h·drawo fpirit of
r,itre : pour this mixture at feveral times, but Cuddeoly,
00
three parlS of oil of lurpeotine, fet for that puryofe
io a glafs baCoo. By a pan here mull be underllood a
dram at leall.
A
moJI violent commotion, acco01p,nied
wilh Cmoke, will i01mediately be raiCed in Ihe liquors,
and lhe wbole will lake fire in ao inllani, flame, and be
cooCumed.
There is not in chemillry a phenomenon more extra–
ordinary, and more furprifing, than the firing of oil5 by
mixing them with acids.
It could never have been
fufpeéted, tha! a mixture of two cold liquors would pro–
duce a fudden, violent, brighr, ,od lalling flame, like
!hat we aJe
al
preCent eonfidering.
'T.
colltbin~
EffinlialOi{¡ wilh Mineral Sulphur.
Balfam
of
S.lphur.
P UT
into a marm one pan of flo\Vm oP Culphur ;
poor on lhem fix pans of the effeOlial oil of turpentine,
for
infl~nce ;
fet the :natras in
~
Cand·bath, and heat it
gradu~lIy
tiJl the oil boi'J.
The fulphur, which at firfl
lay at the bonomof the mmas, will hegin to melt, ,nd
appw tO diffoh'e in the oil. When it hath bni leu
in this
m~nner
for
~bout
an hour, take the matras from
lhe fire, and let the liquor cool.
A
great de.1 of the
flilphur that
w~s
diffol,ed rherein wiJl
fep.,,~re
fromit as
il cools, and fall ro the botlom of Ihe veffel in the form
of Medies, mueh likc a (alt fhooting in water.
When Ihe li'luor is perfeétly cotd, deeant it from the
ful?hl:r lhat lies at lhe bOllom uf the vellCl : tO that
s
T
R
Y.
folphl1r put frefh oil of turpent;ne, lnd procecd a,
bc–
fore: the fulphur will again difappear, and be dir.i,ll'ed
in the oil; bm when the mixlore is eold you will 'inJ
new cryllals of fulpho r depofired
al
rhe bonom. De–
C~lIt
once more lhis oil from lhe cryllals, and pour on
fre!h oil to c1iOiJive theOl: contimlethe (ame mrthod, and
you will fin", that about fixleen pans of effenllal oil are
required to keepone pm of Culphur diff(,h'ed \Vhen cold.
This cumbination is caJled
half"IIIU" Jfulphur iJ tcrebin·
ihinnluln,
if OIade wilh oil of lurpenllne;
anifalUl/J,
ir
with oil of aniCe.feeds; and
Co
of others.
'T, cOlIJbine E/"'li.1 Oi{¡ 'Wilh fixd AllalÍJ.
Slariey'J
s.ap.
TAKE Calt of IRmr, or any other alkali, tholoughly
cakinec1.
He~t
it in a crucihle tiJl il be red, and in that
condition Ihmw it ioto a hot iron monar: rob it quick.
Iy with a very hot iron pellle; aod
?S
fooo as it is pOIV.
dered, pour 00 it, linle by linle, nearly an
equ~1
quan·
tilY of oil of turpentine. The oil will
e~ter
ioto the
falt, and unite intimmly with il, fo as tOform a hud
palle. COOlinue rubbing this eompofition Wilh a 1,ellle,
in ord:r to complet: the union of the two fubllanees ;
and , as your oil of turpentine
di[~ppears,
ddd
m~re,
whieh will unile in
th~
flme
m~nner,
and gil'e a fofler
confillenee to Ihe Coapy marso You may add Jlill more
oil, according to the confillence you intend to give your
~~.
.
Starkey, the firll chemia
w~o
fouild the means of
making (OAp with aneffential oil, and hy whoCe name this
kind of Coap i, rherefore called, made ufe of
~
much more
tedious method than that propofed in Our proceCs.
He
began witb mixing a very fm. 1I quanlity of oil with hi.
falt,
~nd
waited till all the oil unitcd therewith of its own
accord, fo as to difappear entirely, before he added any
more; and thus protraéted his operation exceedingly,
though in Ihe main it was the Came with ours. Theme–
thod here propofed is more expeditious, and was inl'eol'
ed by Dr Geoffroy.
Starkey's foap diffolves in water much as common
foapdoes, wilhoot any CeparatÍllo of (he oil: and by rhis
mark it is knolVn to be well made.
lt
may alfo be de·
compounded, either by dillillation, or by mixing it wilh
an aeid: and il! decompofition, in either of thefe wayl,
is attended with nearly the fame phenoména as the de·
compofition of common [oap.
qr
tbe SlIbjJanw oblaitled
frOtll
VcgrlahleJ
by
mean! o} a grndulltetl Henl,
frOIll
Ihal o} boi/'
illg
Water,
lo Ihe prollgeJI Ibol
CI/Il
be
applicd
lo I/¡em
ir¡
e/oje
Veje/¡.
r.
analifo Vece/tibIe Subjlanw Ihal yicld /leilhu
ti
Fal nor an Effinli.1 Oil. lnjlanced .i/l Cuaíar.m·
.v.,d.
T
AK
~
thin !havings of Guaiacum·wood,
~nd
put them
into a gl. Cs Or f10ne reton, le,ving one half thereof
empty. Set your retort in a reverberating fu rnace, and lute
on a largeglaCs receiver having a fm.1I hole drdled in il,
fucb as is ufed for diflilJiog Ibe mineral acids. Put ;t
JiI'C