e
H
E
M
dull, and look like an eanh. When it comes to have
this appearance. raife yonr fire till the vefiel be red·hm,
and keep it up in this degree till the maller eeare entirely
to rmoke.
enlx of Anlimony reduud loa R(gultu.
Mlx the calx of antimony, which you imend to re–
duce, \Vith anequal quantity of black foap. T his mix–
ture will make a thin pane.
Pnt
it liule by liule into
a
crucible, previoufly made red-hot amidfl live coals.
Thus let the foap burn, till it ceafe to emit all oilyfmoke.
Then cover the crueible ; make the fi re flrong enough to
meh the mamr, and you \ViII hear it efferverce and bni/.
When this noife is orer, let the crucible cool, and then
break it : you \ViII find in it a ueautiful rcoria, marked
\Vith cireles of feveral colours; and under that a buuoo
of regulus, \Vhich is not yet quite pure, aod mun be pu–
rificd io Ihe follo\Ving manner.
Pound this regulus, and mix it \Vith half ilS weight
of
30
antimonial cah, as perfcél ly derulphurated as pof.
fi ble. Put it into a crucible, and cover it: meh the
whole, fo that the fu rface of the mehed maner may be
fmooth and uniform o Let the crucible cool, and theo
break it: you \ViII fi no in it a beauliTul bultonof very
pure regulus, covered \Vith a fcoria, having the appear–
ance of an opaque glafs, or a kind of greyifu enamel,
moul,led
00
the fioelyradiated furfa';e of the regulus.
;/nlil/lony calcind wilh Nilr(. Liv(r of Anlimony.
PULV ElI
SE
and mix
pcrf~é\ly
together equal parlS of
nitre and antimony: pllt the mixtu re ioto ao iron mor–
tar, and cover it IVith a tile, which ho\Vel'er alUn not
fuut it quite c1ofe. With a live coal fet fire to the mat–
ter in lhe monar, and imm"diately withdraw il. The
mixture \ViII Aame, with great
d~tonation;
which being
overo and the mortar cooled, inren it, .nd nrike its
bouom to make all the matter fall out. Then, by a
blolV with a.hammer, feparate the fcoria ftom the fuining
pan, which is ihe
liwr
of
«ntimol'J.
Anolh(r e.leinali.n
of
Anlim.nywilh Nilre. Diophl–
n lic Anrilll'ny.
Mlx one part of amimony \Vith three pans of nitre;
projetl this mixture by fpoonfulls ioto a crucible kept
red hot io a furnace. Each projeélioo will be auended
IVith a detonation. Continue doing this till yon have
uf"d all your mixture: lhen raife the fire, alld keep it
up for tWO hours; after which throw your matter into a
pan fu ll of hot water. Let it lie lleeping io water kept
hot for a whole day. Then pou'r off the liquor: IVafu
the \Vhite powder you find at bOllom io warm water ;
and repeat the ablutions till the powder become infipid.
Dry it, and you bave
dtaph+rrlic onlimony.
ealx
of
Anril/lony vilrifd.
T ARE any quamity you pIcare of calx of antimony,
made without a<idition; put it ioto a good crucible.
which fet in amelring furnace: kindle the fire gradually,
aod leal'e the crucible uncovered at the beginning.
A quaner of ao hour after the mauer is red-hot, co,
ver the crucible, and excite the fue vigoroufly till the
s
T
R
Y.
cnlKmelt. You may know when it is thoroughly melted,
by Jipping into the crucible an iron wire, to the cod of
which a linle knob of glafs will adhere, if the matter be
in perfel! fufion. Kccp it in fufion fo r a quarter of aD
hour, or wher longer if your cruciblecan bear it. TheD
take it out of the furnace, and immediately pour out the
mehcd matter on a fmooth none, made very hot for the
purpure: il \ViII prefently fix into a yellow glaf9.
Kml/u
Min(ral.
BREAK any quantity you \ViII of Hungarian antimooy
into little bits: put it into a good eanhen eotree-pot :
pour
00
it twice its weight of raio-water, and
a
fourth
pan of its weight of IVell filtered liquor of nitre fixed by
charcoa!. Boil the whole bri/kly for twO hours, and
then filter the liquor. As it cools it will acquire a red
colour, grow turbid, and leave a red powder
00
the
fiher.
Returo your amimony iota the coffee-pot. Pour
00
it as much rain-water as before, and three founhsof the
formerquantity of the liquor of fixed oitre. Boil it
i–
gaio for two hours, and then fiher the liquor.
Ir
will
agaio depofite 'a red fediment. Return your aotimony
into tite coffee pot : pour on it the fame quamity of rain–
water, and half the fir(l quaotity of the liquor of fixed
oitre. Boil it agaiu for twO hours, aod filter the liquor
as formerly. Wafu all thefe fediment! withwarm water,
till they become infipid; then dry tbem, aod you have
the
Rumu minual.
R(gulu/ Df AnlimMJ difo!V(d in Ih( Minua! Acid/.
COMPOUND ao
oqua " gú
by mixing together four
meafures of fpirit of nitre, and ooe meafure of fpirit of
falt : on a fand-bath moderately heated place a matras,
into which pour fixteeo times as much of this
oqua r(git
as you have regulus to dilfolve. Break your regulus io
liule bits; aod throw them fucceflively one after another
ioto lhe mmas, obferving oot ro add a new one till that
put in before is emirely diifolved: continue this till your
regulus be all ufed. By degrees, as the dilfolutioDad–
vances, the ¡¡quor will acquire a beautiful golden co–
lour ; which however will infenfibly difappear, as Lbe
white fumes that contioua/ly afcend from it evaporate.
R(gu¡'1J of Anlb"ny cOl/loinrd wilh Ih, AcMofS(ajoll.
Bull(r
of
Anlimony. Cinaoar
of
AnlilllOl'J.
PULvER rSE and mix thoroughly fix partS of reglllus
of amimony, and fixteen partS of corrofive fublimate Put
this mixture intoaglafs reton that hath awide fuon neck,
and let one half of its body at lea(l beleft empty , Set it
in a reverberatory furnace, aod having fitted a reGipient
tbereto and luted the joint, makea very fina/I fire at fira
tO heat it flowly. Increafe it afterwards by degrees, till
you fee a liquor afcend from lhe reton that grows thick
as it cools. Keep up the fire to this degree as long
as
you fee any of this malter come overo
When no mOre arifes with tltis degree of fire, unlute
your velfds, take otr .he receiver, and io its place fub–
lIitute another filled with water. Then increafe your
fire by degrees till the reton be red-hoto SOllle run-
niog