e
II
E
M
h~iog
dooe.
incre,\f~
YO'1r
r.refo al lOmakr
, h~ v~r.;
i
cowioing Ihe fand·¡',nh red ·ho!. lo
Ih~
a;<.n\.::
JOU
\\'ilI !ind a c,lx of nlvcr. which mnll be Oldled io arlu–
cible l'Iilh fOl1le foap ano ca\cineo \Vioe· lm.
If
Ihe dinill::!ioo be Oopptd wheo pan of the pbl' í":l
is drawo off, aod Ihe liq'Jor be Iheo f"ffcred
to
c,)ol.
many cryOals will thoul lhmio, which are a ocm,.1
tAl!
cootlilllted of the oi!rous aeid aod Cilver.
If
Ihe dillil–
Jadoo be carried fUrlh er, and Ilorpeo wheo oear ils con–
e1uCioo, the liquor beiog Iheo f,,["red 10 cool \ViII wholly
coagulate iOlo a blackith ",.fs c.lled Ihe
i'1<1/1.11
jlOIIC.
70
flpartl l' Silver froJ/llh: nilNUI Acid by P",itilo-
lion,
Lun. Coroea. Luna Coroea
(cJuccd,
INTo your folulion of filver pour
a~NII
a founh parl
in weight of fpiril of fah, folulion of fedal!, or ful ,,!ion
of fal ammoniae. The liqll<>r wiil ioOandy beeome tur–
bid and milky. Add t"'iee or
thri~e
ilS w(ighl of f,ir
water, and let il Ibnd fome fome hours ro fmlt.
It
\ViII depofile a while powder. DecaOl lhe cbr liquor,
and on the precipilate po", freOI
fl11/a
[orlÍ! ,
or fpiril of
fah, aod wal'm Ihe whole 00 a 1311d b.llh Wi,:l a geode
heal for fome time. Pour off Ihis feecod liqccr, aod
boi! your
precipilal~
io pure wmr, Olifliog it f(vm l
tintes, till the precip:tate aod Ihe water be bOlh quite
iofi pid. }'ilter the whole, aod dry the preeipitate, whieh
will be a
1111/1 COf/Ufl.
aod muO be reduced in Ihe fol·
lowiog maoner.
Smear the iofide of a good erueible well with foap,
Put your
luna cornea
ioto it; cOI'er ie with half in
weight of falt of tartar, thoroughlydried and pulverifcd;
~refs
the whole hard down; pour Ihereoo as much oil, or
melted tallow, as the powder is capableof imbibiog ; fee
the crucible thus chargrd, aod clofe covered, in a,mele.
iog furoace, aod, for the firll quarttt of an hour, kindle
no more lire than is oecelTary to n\1ke the crueible mo·
derate!y red; after that raife it fo as 10 OIeh the filver
and the fa h, Ihrowiog iOlo Ihe crucible
Irom
eime
10
time little bits of tallolV, Wheo it-
ceab
to finoke, let
the whole cool; or pour it into a hollow iron cone,
warmed and tallowed.
70
dijolve Si/ver, and flfar.', il Irolll Cold, hy
Ce-
71J~n/rJlion.
MIX thoroughly together
lio~
hriek·dull fou r pans,
vitriol calcioed to rednefs ooe part, aod fea-fale or oi–
tre one pHI. Moincn this pOlVder with a linle water.
With this cement cOI'er the bonom of a crueible half ao
inch thick; on this CirO bed laya thin plate of Ihe mafs
of gold and filver you iotend tO eemenl, and IVhieh )'OU
mua previouOy t,ke care tO beat iato fuch Ihio plates.
Cover tltis pl,tte with a fecood layer of cement, of the
f.1me thickoe(' as the former; on Ihis fecond bed lay an–
other plate of your melal; eover il io like maooer wilh
cement; aod fo proceed tiJl thcCIucible be filled tOwilh·
in half an ioch of ils brinL Fill up the rcmaining Ipace
",ith cement, .nd clnfe Ihe e,.ucible with a cover, IlIted
wilh a patle made of Windlor·loamand \\'ater : Se, yOllr
crucible thas ch"ged in a furnaee, whofe fire'
pl.ceis
deep enough 10 let it be enlirdy furrounded with co:tls,
~uite
up 10 ilsmoulh, Light fome eoals in the furnace,
s
T
R
Y.
" ,~ir.~
cm OOt eo make Ihe fire
~ery
briOl al firn; io–
creal ~
it hy degrees, but only fu far as :0 mr,ke the cru–
cible nlOCJ..
rr.dyred ; keep ur lhe fire in Ihis oegree for
.cighteen or ll'lenty hours : Then lu Ihe
fi" ,
go OUI; o·
I~_n
Ihe crucible \'Ihen ie is cold, and feparale the ament
Irom you,. plates of gold. Boil Ihe gold repcatedly in
fair WdlCr, lill the "'''ter come off quite iofipid.
O[
e
o
P P E R.
7. h "lral' C'Nr!'
Irom ill
Orto
llEAT
yonr corper ore
10
a Cine powder, flaving firll
freed it as aeeuralely as roffible, by waOling and roaO–
ing, from all nony, eanhy, fulpbureous, and arbieal
pam , M,x )'our ore thus pulverifed with Ihrice its
weight uf the hlaek flux; pttt the mixture intn a eruei–
ble; cOI'er ie wilh cOOlmon fale to the thieknefs of hall
an ineh, aoo prefs lhe whole dolVo IVith your finger.
With all this Ihe erueible muO be but h,llf full. Set ie
in a melting furuaee; kindle the Cire hy d' grees, and
ri.if~
it inftnfibly liU you he.r the lea·ralt crackle. Wheo
the derrepiminn is Ol'er, make the crueible moderately
red·hot fur half • quaner of atl hour, Then gi,'eaeoo·
fiderahle degree of heat, exeit;og the fire with a pair of
good perpelual bellows, fo tbat the crucible may become
very red hOt, aod be perfdtly ignited. Keep the lire
up
10
this degree for aboue a quaner of ao !¡'our ; then
take oue Ihe erueible, and with a haminer n,ike a few
blolYs on the Ooor 00 which you fet it, Break it ,.heo
cold.
If
,he
~pemioo
hath been rightly and fuectfsi'ully
performed. you will find ae Ihe bonom of the rellel
,1
Iwd
regulus, of a hright ycllow colour, aod femi-m,dl"ble;
and ol'er it a fcori,1 o; a yelJowilh browo colour, hard,
aod Oliniog, from which you may feparate the regulus
wilh a hammtr.
70
pllrify Macl
C'N1r,
alld rcnder
ir
mall,abl,.
BR EAK
inlo fmalJ bits che blaek copper )'OU iOleod
to purify; mix therewi,h a lhird pan in weight of
granulatcd lead, and put the whole iOlo a cupel fet uo–
drr lhe muIRe ina cupdling furnaee, ar.d prel'iouOy heat–
ed quite red, As roon .s the metals are in lhe eupel
raife Ihe fire eonliderably, making ufe, if it be ueedful,
of a pair of perpetual bellows, to melt Ihc eoprer fpeedl'
Iy. Whenit is thoroughly mdted, 10ll'er the fire alillle,
aod cOOlintle it jull high eoough
10
keep the metaJline
mafs in perfeé! fufiuo, The melted ,"aeter will then
hoil, aod Ihrow up fome feori:!!, which \ViII be
abfor~ed
by the cupe!.
When mon of the lead is eonfumed, raire
th~
fire a–
gain tilllhe raee of the eopper beeome bright and Ihioiog,
therclty fllewing that all ilS alloy is feparaled.
.~s
foon
as your eopper comes to this tlate, cOI'er it \\'ith ehar–
eoal duO conve)'ed ioto the eupel lI'ith an iroo laddle:
Then
ta~e
thecupe! out of the furoaee, aud let it cool.
70¿,prive C'N" 01
ill
Phlogij/oll
kv
C.lcinalior.,
PI'T
your errper in filints ioto a tell.
a~d
fet it no–
d" themulllc of a cupclling furnaee;
li~ltt
lhe firr, and
keep up fueh a degrcc of btat as ma)
mJ~e
the II'h-"le
~u¡:e