e
H
M
1110fe employcd lO draw Ihe odoriferous walers and
elrenlial oils ol" plants are gcnmlly made of cupper, and
confill of feveral piem. The fid!, which is dcligned lO
contain Ihe plant, is formed nearly like a hollow cone,
Ihe. vertex whereof is drawn out in Ihe !hape of a hollow
cylinder or tube: This pan is named Ihe cuburbil, Plate
LXIV. fig.
l .
A; and ils tube Ihe oeck of Ihe alembic
B.
To the upper end of Ihis tube anolher veiTel is foldered :
This is called Ihe head
C,
and commonly has likewife
Ihe form of a cone, joined to the neck of the alembic by
ils baCe, round which on the iofide is hollowed a fmall
groove communicating with an orifice-Ihat opeos at ils
niofl depending parto To this orifice is foldered
a
fmaH
pipe in a direé!ion Oopiog downwards, which is called the
ooCe, fpout, or beak
O
of the alembic.
As foon as the malters contained in Ihe alembic grow
hot, vapeu,", begin lO arife from them, altd aCcending
through the neck ofthe alcmbic into Ihe head, are by
the fides Ihereof flopped and condenfed: From Ihence
they trickle down in little Ilreams to Ibe groove,
whi~h
cóaveys them to the (pOUI; and by that they pafs out of
the alembic into a glafs veOel or receiver
G
wilh a long
neck, Ihe ead of the fpout being inttoduced inlo that
oeck and luted !bereto.
To facilitale the refrigeration and condenfation of Ihe
vapours circulaling in the head, aH alembics of mml are
niareover provided witb another Jliece, which is a kind
of large pan of the fame metal, fined and foldered round
dte head. This piece ferves to keep cold waler in,
Which incelraatly cools the head, and Ihmfore it is call–
ea Ihe refrigeratory
E.
The water io the refrigeratory
itfelf grows hot after fome time, and mufl Iherefore be
changed occafionally; the heated waler being Dril drawo
off by meaos of a cock fixed near the bonom of the re–
frigeralory. AH copper alembics Ihould be tinned 00 the
iófide for the reafons already given.
When faline fpirits are to be diflilled, alembics of me–
tal mufl not be ufed; becaufe the fal ine vapours would
corrode Ihem. In Ihis cafe recourfe mufl be had tO a–
lembics of glafs. Thefe confifl of pieces only; oamely, a
eucurbit, whofe Cuperior orifice is admitted into, aod ex–
aé!ly luted with its head, which is the fecond pieee.
In geoeral, as alembies require that the vapours of
the maner to be difliHed !hould rife to a eonfiderable
height, Ihey ought to be ufedonly when the mon volatilc
priociples are to be draVlo from bodies: And the lighter
and more vol.tile Ihe fubflances to be feparated by diflil–
lation a:e, the taller mufl Ihe alembie be; becaufe the
mofl ponderous pans, beiog IInable to rife aboye a cer–
tain heighth, fall back again into the eucurbit as foon as
theyarrive mere, leaving the lighrer ro mount alone,
whofe volarility qualilies Ihem to areend ioto the head .
When a maner is to be diflilled Ihat require! a very
tall alembic, and yet does not admit of a metalline ver.
fel, the cnd will be befl anfwered by a glaCs velfe! of a
round or oval!hape, having avery long neck, with a{mall
head fiued to its extremity. Such a velfe! ferves many
purpores:
lt
is fometimes employed as a receiver, and
at other times as a digefling velfe!; on which lall occa–
Jion it goes under the name of
a
matrafs, lig.
3.
Wheo
VO~.
n.
No. 34'
'3
s
t
n
Y.
)'09
oncofthefe provided wirh ahead,
(lig.
3.
Cl,
ía .pplied
to Ihe purpufe of diflilling, it forms a ron of alembic.
Time are fome alembics of glafs, blown in fuchaman–
ner by the workmen, thar Ihe body and he.d form but
one continued piece. As IheCe alentbics do not fland in
need of having their femal
~iem
IUled logether, they
are very IIfeful on fome oecallon!, when fuch exeeeding
fubtile vapoor! rife as are capable of tranfpiriog through
lutes. The head mul! be open at the top, and provided
wir~
a !hon tube, through which by mean! of a funoel
with a long pipe, Ihe maner to be diflilled may be io–
troduced into the cucurbit. This is to be exa/lly clofed
with a glars flopple, the furface whereof mufl be made
to fit the infide of the tube in every p'Oinr, by rubbing
thole t\Vo pieces well together with emery.
Another fort of alembic hath alfo been invented,
whieh may be ufed wilh advántage when cohobation i.
required; that is, when Ihe liquor obtainedtby dinilla·
tioo is to be returned upon the maner in the cucurbit ;
and efpeeially \Vheo it is intended that this cohobation
!hall be repeated a great number of timeS. The veife!
we are fpeaking of i! conllrué!ed exaé!ly in the fame
manner as that lafl defcribed; excepl that its beak, in–
flead of being in a flreighl line as in Ilie other alcmbics,
forms acircular arch, and re·entm the eavity of the eu·
curbil, in order to convey back again the liquor colleé!–
ed in the head. This inflru!1lent hatb commonly t\Vo
beaks oppofite to eaeh other,
bo.thlurned in this manner,
and is called a
p,lican
:
11
faves the artifl Ihe trouble of
freqttently unluting and reluting his velfels, as well as
the lofs of a great many
vapour~.
There are cenain fubJlances which in diflillation af·
ford mancrs in a concrete form, or rire wholly in the
form of a veíY light powder, called
flO'WU/.
When
fuch fubf!ances are to be diflilled, the eueurhít which
cootaios them is eovered with a head without a nore,
which is named a
Mind·h,ad.
When the flowers rife in great quaotilies
~nd
very
high, a number of heads is employed to colleé! them ;
or rather anumber of a kind of pots, eoofifliog of a
oo·
dy only without any bottom, which fitting one into the
other form a canal, ihat may be lengthencd or !honenell
at pleafure, according as the flowers to be fublimed are
more or lefs volalile. Thelafl of the heads, which ter·
minates the canal, i! quite clore at one end, and makes
a true blind·head. Thefe velfcla are called
a/udili:
they are ofually of eanhen or none ware.
AII the velfe!s ahove mentioned are fit only for di·
flilling ruch light volatile matters as can be eafily raifed
and broughl over; fuch
as
phlegm, elrential oils,
fra·
grant \\-,ters, acid oily fpirits, volatile alkalis,
&e.
BUI
when the point is to procure, by dinillation, principies
thal are mueh lefs volatile, and incapable of rifiog high,
fuch as the thick f.tid oils, the vitriolic, the nitrous, and
the marine acids,
&c.
we are under a neceffity of haviog
reeourre to olher velfels, and another manocr of
di·
flnling.
Ir
is eafy to imagine, that fuch a velfe! mufl be much
10IVer than the alembic. Jt is indeed no more than a
hoJlo\V globe, whofe upper pan degenerates inlO
a
neck
:t
2
E
or