110
e
H
F.
M
or lube, that is beot ioto ahorizootal pofilioo
j
for which
reaCooIhis ioílrumeol is called a
re/orl:
11
is always of
ooe fiogle piece.
The mauer to be diílilled is iOlroduccd iOlo Ihe body
of Ihe retor! by meaos of a ladle wilh a loog lubular
Ibaok. Theo il is Cel io a faroace built purpoCely for
this uCe, aod
Co
Ihal Ihe oeck of Ihe retor! comiog OUI
of Ihe furoace mRy, Iike Ihe Ihe ooCe
oC
Ihe alembic,
{laod io a 1I0ping pofition, 10 facililale the egreCs of
tbe liquors, 'which by ils means are conveyed 10 a re·
ceiver, iOlo \Vhich it is iOlroduced, and wilh which it is
IUled. Tbis way
oC
diíliJling, in which Ihe vapours
feemralher lO be driven out of the vell'e1 horizonlally
and lateraJly, Ihan raiCed up and fublimed, is
ror
that
reaCon caJled diílillation
pir lalul.
Retom are, of all the inílruments of diílillation,
1hoCe that muíl Cuílain Ihe greateíl heat, and refiíl Ihe
Ilrongell Colvenls
j
and therefore Ihey mul! nOI be mlde
gf melal. SJme, however,' which are made of iron may
do well enongh on cenain occafions: The ren are eilher
gf glafs or earrh. Thofe of glaCs, for the rearons aboye
given, are preferablelOIhe olher Con, in all caCes where
tbey are not 10 be expored 10 Cuch a force of fire as may
mell them. The bel! glafs, Ihat which ílands bOlh heat
20d ColveOls beíl, is thal in which Ihere are feweíl alka·
line Calls: Of this Con is Ihe green Germao glafs: The
beauliful white cryílal glafs is far from being equallyfer.
Ticeable.
Relons, as well as alembics, may be of difFerent
forms . For example, Come malters are apt to Cwell and
rife over Ihe neck of Ihe relOr! in Cubílaoce withoul fuf·
fering any decompofition ; when Cuch mauers are to be
diíliJled in a retan, il is proper that me body of Ihe
veC·
fel, inílead of being globular, be Jrawn out iOlo the form
gi a pear, fo as oearly tO reCemble that of a cucurbit. lo
a retort oí Ihis kind, Ibe diílance between the bouom
and the neck being much grealer thao in thoCe whofe
hodies are Cpherical, Ihe maltCrs contaioed bave much
more room for expanfion;
Co
that the inconveoience
iJerc meOliooed is Ihereby prevented. RelOrts of this
form are caJled Englifh re10m : as Ihey hold Ihe mido
.ue place belween alembics aód common lCIons, they
l)Iay be uCed 10 diniJl Cuch matters as have a mean degree
gf volalilily belween the greareíl and the leaíl.
It is moreover proper 10 have in a laboralory Cundry
relom wilh necks of differenl diamelm. Wide necks
will be found lhe fineíl for conveying thick matters, and
fuch as rcadily become fixed
j
for inílaoce, fome very
tbick felid oils, bumr of aotimony,
&e.
for as Ihefe
maners acquire a confiíleoce as foon as they are out of
the reach of a cenain degree of heat, they would fooo
tbo,k up a narrow neck, aod by ílopping Ihe vapours,
which riCe al the (ame time from the relOrt, mighl occa·
fion Ihe burfling of tbe vell'e1s.
Sorne retom are alfo rnade witb an openiog 00 tbeir
llpper C!.de, like Ihat of tubulated glaCs alembics, which
is 10 be c10Ced io Ibe Came manoer wilh a glaCs ílopple.
TheCe retorlS are alfo called
I,ubulaud rtlDrll.
and oughl
alway\ to be uCed whenever it is necell'ary to iotroduce
(ren¡ matter into Ihe reton during Ibe operatioñ; feeiog
it
may
be
dODe
by
mew
of lhU\mvenúoD, wilbout
uo.-
s
T
R
Y.
IUliog aod reluling the vell'els
j
which ought alwayr-10
be avoided as much as poffible
One of the thing< thal moíl pcrplexes Ihe cbemills is,
the prodigious elafticilY of
Im.nydifferenl vapours,
whic~
are frequently difchargcd ",ilh impeUlofit)' dnring Ihe di·
llillalion, and are even capable of buríling the vcll'e1,
with explofion, and with dangcr lO Ihe anill. On fuch
occafions il is abfollltely oecefl:1I y to give Ihefe vapours
vent, as we (hall dire[t in ils proper place: But as Ihat
can never be done Wilhoul lofing a great maoy of them;
as Come of Ihem io panicular are
Co
elaftic, that fcarce
aoy at allwould remain in tht vell'e1
j
for inllance, Ihofe
of the Cpiril of nitre, and eCpecially thofe of the Cmok¡ng
fpirit of falt : Ibe pra[tice is to make ufe of very large
receivers, of abollt eighleen or l\Venty ioches diarnerer,
tbat the'vaponrs may have fuflicienl room10 circulale io,
and, by applying ro Ihe \Vide Currace prefenled Ihem
by
the extenfive infide of Cnch a Iarge vefrel, may be con·
denCed ioto drops . Thefe huge retelvers are cummooly
io the form of hoJlow globes, aod are called
ha/lonl.
To give theCe vapours fhll more rOo.l1, ballons bave
beeo contrived wilh I\VO opeo gullels in each, diamelri·
cally oppofite lO one anolher : wbmof one admil! Ibe
neck of the retan, and the olher is received by one of
the gullels of a Cecond bailon of Ihe fame form, whicb i1
joioed in like manner 10 a lhird, and' fo oo.
By
tbis aro
tifice Ihe fpace may be enlarged at pleafure. Thefe bal·
lons with two necks are called
adGPlm.
Operalioos on bodies Ihal are abColutely li1<ed. as me·
tals, nones, fand,
&c.
require only fuch vell'els as are
capable of conlaining thoCe bodies aod refiíling the force
of fire. TbeCe vell'els are lirtle bollow POI!, of diffe·
rent dirnenfioos, which are called crucibles. Crucible,
can hardly be made of any thing bUl canb; Ihey o¡'ght
to Ime a cover of Ihe Came malerial
fimo
10 fhut Ihem
cloCe. The beíl earth we know is Ihal \lIbereor thofe
pOIS are made
m
which bUller is brought from Bretagne:
TheCe pots themfelve, are exceeding good crucibles
i
aod
tbey are almoíl Ihe only ones Ihal are carable of holding
glaCs of lead in fufioo, wilhoul being p'enetrated by ir.
For Ibe roafling of ores, Ibal is, freeing Ihem by
tbe help of fire from their Culphureous and arCenical
pans, . Iillle
~ups
made of Ihe Came malerial wilh cruci·
bIes are ufed
j
but Ihey are made !lal, fhallow, and wi·
der aboye rhan be.low, Ihal Ibefe volatile mallers may the
more freely exhale. Thefe .ell'els are called
lifiJ,
or
fcoriftm ..
They are fcarce uCed bul iD Ihe
docimalli~
an, thal is, io rnakiog Cmall all'ay! of
ores.
7he Theory
q(
crmjlru8ing
the
FurnaceJ
moft
commonly ufro in Chemijlry.
SKILL in conduéting aod applyiog tire properly, and
delermining its difFereol degrm, is of very
g~eat
cooCe·
quence 10 the fuccefs of chemical operations.
As il is-exceeding dillicull 10 govern and moderale tbe
a[tion of fire, wheo Ihe vdJ'ds in wbich any operatioo i,
performed are imrnedimly expoCed to il, cbemiíls have
contrived to convey beal to their velTels, in nice opera.
tions, tbrough dtffereol Olediums, wbich they place
oc~
cafionly
betwccn
tbofe
ve1fels
aIld
Ibe ÚIe.
TJ¡of'c