e
H
E
M
"hich they
~ct
rid of bY'
ro~ning
it. After this thcy
fl crp the
c.lcin~d
none in
w~tcr,
wl ich dilrol,es the aJum
it cont.ios, aod to this folulioo they add a certaio
qOln·
tit)'
~f
a
I)'e 1Il00de
01
thc .fhcs of fea·weeds.
r . a Iran Ih, Vil
ri.li, AcMIr.mCrun Vilri.l.
T AKE any quanti ty uf greco vitriol : put it iD ao
\lo~lnlo
earlheo vefl'e1, and beat it gradu.lly.
V~pou"
will fooo begio tO rife. lom afc the lire
~
liule, aou it
" ill liquify by
m~aos
of thc wml cootained in it, and
acquirc ",hat we calltd ao
a9u~,u,
I".r.
Cootio"e Ihe
~~lcinatioo,
aod it lVill becllme lefs . od lefs fluid, gro
IV
thiek, aod turo of a greyilh eol"ur. Now r.ife your 6re,
. od keep it uptill the f. /t recover its folidity, aequire
~o
or.oge eolour, aod be::io to grow
re~
whae it i,"me–
dimly touehes the Gdcs uf the ve(fd. Theo take it out
.nd reduce it tO powder.
PUt Ihe "itriol 1hus ealeined and pulverired iOlo
a.
good eanhen T<lort, of whicli one h. Jf al leaHmull re·
main empty.
S~I
the mort in a re,'erberatory (urnaee:
}'it therelo a
I~rge
gla(s reeri"er, and, having luttd the
joint \l/tiI, give [¡re by dctrees
You will (oon fce
white clouos rife ioto the reeeiver, which will render il
opaque alld heal il. Continue the fame d<gree o( fite
lill lhefe clouds d.f' rpear:
T~ey
\ViII be fucctcd:d by a
liquor IVhich wiJl tri.:kle down lhe Gdes of lhe rceeiver
in
veins. $Iill keep up thc lire
10
l~e
fa me degrce as
JJn~
as thefe
"dos
app~ar.
When lhey begin to abale,
enereafe the lire, and rufh il tOthe ulOlofl eXtremilY :
Uponlhis thcre \I'ill come over a black, thiek liquor : It
\ViII even be found conge.led , and preve the iey oil of
vilriol, if eare halh been l. ken
10
change lhe receiver,
keep the ' efl'els perfeél!y c1ofe, anu give a fufficieol de·
!\ree o( heo!. Proeced lhus tiJl nOlhing more comes o–
ver, or at leafl . ery hule. Let the ye(fels eool, unlute
lhem, pour the
C"Ot~OIS
of the recei' crinlo abotde, and
feal il hcrmelicaJly.
r . tluo/llP1' Sulphur, ami ,x/r.n ill AcM,
6)
hurn–
ing 'l.
TAK
6
anyq'Jantity of lhe pu refl fulphur;
611
thmwith
acruc.ble or other eJrthendiOt ; hm it liJl it mdts ; lhco
fL!
.1
on fire, and when
liS
wholefurface is lighted, place
it un,ler
a
large glars head, fo lhat the Rame of the (ul–
phur do not louch cilher its fijes or bouom; lhal lhe
alr hJve fICe accefs, in arder to
m.kelhe fulphur burn
de.,: lhol: lhe head incline a liule loward Ihe fide on
\l/hich itl beak is,
11m
as thc vapoulS eondenfe ,herein
tite
h~"nr
mJy run off with eafe. To lhc uc,tI¡
o(
thi,
vefi.1 fil a receiver : The fu mes of the lighled fuJphu r
lIIill be eooden(Ld, and gatlter ioto drops in lhe head,
out of hich lhey \l/iJl run iOlO Ihc " ceiver. Th<re,
\1
hen the fulphur has done burninn, you \l/IJl 60d ao acid.
liquor, which is lhe fpiril
o(
fulphur.
r . "r.unlra/( Ih, Vilri.lic ,Ieitl.
T A
lB
the "ilriolic
¡cid
you inlend to concenlr:tle,
lh" is, to dephlegmale and make flrunger: Pour it inlo
a
g"od Rlafs
retOr! 01
fuch a fize lhal your quanlity of·
¡cid
ItMy
bUI hJlf
6J1
il : Set lhis reton in lhe faod–
bnh of a rcvcrbmllog furnace ¡. 61 it
10
a receim ;
s
T
R
Y.
J"le it on, and give a gradual fire. Tliere will come
o"er into the receiver a clear liquor, the {¡rn drops oE
which ",iJl be bUl faiolly acid : This is lhe mofl aqueou,
pan.
Wlten lhc drops begin to follow one aoolher mueh
morc Oowly, raife your fi re, tilllhe liquor bCfintobub–
blc a I:ttlc in the middle. Keep il thus gently.boiling•.
liJl olte halr or tlVO lhirus ¡hereof be come over inlo lhe
recei"er. T hen lel your ,'cfl'ds cool ; unlute them'
Wh. l rem,ins in the rClon pour inlo acryfial bOlde, aod
flop il exaélly
w~th
a glafs fiopple rubbed. with emery,
r. tltcDmpafe vllr¡"fa/er! r arlar
6,
m,anl
of
Ih, PhI.-
giJ/on; or
,.
w npofe SI/Iphur
&,
c01l/bining Ih, Vi–
/ri.lic Aeitl wi/h Ih, Phlogif/on.
TA ~
I
equaJ pans of vitriolaled tartar, and
,rry
dry
falt of lartar, (eparately reduced to powder; add an
eighlh part of thcir wcighl of charcoal dufl; and mil!"
lhe whole together very accurmly, ThrolV this mix.
lure into a red·hot cruciule, placed io
a
furnace fillee!.
Wilh burning eoals. Cover it , ery dofe, and keep ir
very hOl, lill the mixlure mcll, \l/hich may be knowQ
b), uncoveriog lhe crucible from lime to lime. There
will thenappear a bluifh flame, accompanied with a PUli–
gcnl rmell of fulphur.
T.kethe crucible out of the fire; di(fol.e its can"
lenlS in hOl waler; fiher the (olulioo tb'rough brown
paper fupported by a glafs fun nel ; drop ioto the fi her–
ed liquor by little and lillle any acid whatever. As you
add lhe acid, lhe liquor will grow more and more tur.
~id.
and
I~t
fa!1a grey.
precipi~m..
Conlinue droppiog
lO
more aCld
1111
Ihe liquor wdl y,eld no more pr<cipi–
tate. Filler il a fecond time
10
(eparate it from the pre–
cipilarc : What remain! on the lilter is
a
true infia.m–
l}l.ble fulphur, wbich you may ejlher mell or fu b–
lilOe into fiowers.
01
tbe
ITROU S ACID .
r o rxlran ni/re Oul
of
ni,,.., ,arlhJ gntl fionu.
'{h,
purifwion
of
1.1t
p,I". MOI6"
'1
nil" , Mag–
ntjia.
TAKE any quantity o( nitroul eanhs or fioDes; re–
duce lhem
10
powder; and lherewilh miK a lhird pare
of the afh es of grten wooo and quiek.linte. PUl lhis
mixture iOlo a barrel oro
" 1,
and pour on it hot waler
10
abOUl lwice lhe ..eighl of lhe whole mafs. Let il fiand
thus for tWeOly four houlS, fli rriog it frolTl" time to lime
Wilh a lIick. Then fi/ter lhe liquor lhrough brown pa.
per, or pafs it th rough a ft.r-nd bag, till il come cica"
it will then
ha~e
a yellowifh eolour. Boil Ihis liquor,
and e.aporate
1111
yO\)
perce.ve11m
a drop of it lel (all
onanyeold bodyeoagulates. T hen fiopthe <faporalion
and let your liquor in a eool place• .Inlhe fpace of fou;
and lwenly hou" cryltals will be forroed in il, lhe 6gure
of whlch is that o( an hexagooal prifm, having its oppo–
fi te planes generally equa!, and lerminaled
at
eaeh ex–
lremity by a pyramid of lhc faroe oumber of fides. Thefe
eryll.JswIII be o( a browoifh colour, and deBagrate on a
Ji"e coJo
Oleanl lhe liquor [rom tbcJi cryfials
i
mjx jI with
twitC