e
H
E
M
bitumens. This oi! alfo will be accompanied with an a·
q'leous acid liqudr. In the reton will be left a charred
maner, which, being put into an ignited crucible in the
fire, burns (or fome t.ime, and, w.hen well caJcined, leave,
; white earth .
The liquors that rife firll in this dilllJlation, and which
\Ve direaed to be kept by thcmfdves, are a mixtijre con ·
filling,
l .
o( a
high.Jydephlcgmmd fFirit of wine, of a
mofl (ragrant fmell;
2.
o( rether, which the (pirit o(
\Vine wherewith it is united ,.enJers mifcible ",ith water;
3. o( a portion of oi.l, which commonly rifes with the
;ether towards the end of the operation; 4. and fome·
limes of a linle fnlphurcous acid, i( the recelver be not
rhanged (oon enough.
In order tO feparate the rether from thefe other fub–
Ihnees, put the whole iotO ao Englilh retort, with a lit–
Ile oil of tartar
p(r ,UiqlliunI
to abCorb the fulphureous
acid, and diflil vcry OOlVly in a fand bath hemd by a
hmp, tiJl near half the liquor be come overo Then ceafe
rlill,Jling; put tbe liquor in the receiver intO a phiallVith
f~me
water, and Ihakc it ; you will fee it riCe with ra·
pidity to the upper pan of the phial,
~od
fio1t on the furo
face o( the water : this is the rether.
Spiril o/lVint ,.mhin,d ""ilh Spiril
.¡
Nil".
S,",<el Spiril o/ Nil".
lNTO an EngliO\ reton o( cryllal gla(s put fome high·
Iy reai!ied (pirit of wine; ,od, by means of a glaCs fu o·
n.e1 wilh a long pipe Ict (all into your (pirit of wine a
few orops of the C,noking Cpirit of nitre. There wiJl
ari(e in the reton an efl'uvefcence anended with heal,
rfd vapours, and a hiffing noife like that of a live coal
quenchcd in wmr. Shake Ihe velfel a linle, lhat the
liquo" may mix thoroughly, aod thal the heat may be
equally communicmd tO lhe whole. Then add more
fpirit of nitre, but in a very (mall quantity, and with lhe
f.meprecautions as be(ore. Continue thus adding fpirit
of nitre, by linle and linle at a time, tiJl you have put
into the reton a quamily equal to a Ihird pan o( your
fpiril of lVine. Lel Ihis mixture fland quiet, io a cool
phce, for ten or twelvehou,.!; theo (el il tO digefl in a
very gcnde warmtb (or eight or ten days, baving firfl
IUled on a reeeiver tO Ihe retort.
During ihis time a
fm.JIquanlily of liquor ",iJl come
over
intu Ine receiver, whieh mufl be poured back into
Ihe retort. Then diflill with a (omeIVhat flronger de·
grce of heat, bUI flill very gemly, till nOlhing be left io
tbe relOr! bOl a Ihick matler. In the reetiver you
will fiod a fpiriluous liquor, of a quiek grateful (mell,
which wiJl excite a veTy Cmarl (en(alion
00
the longue,
hut without any corroGve aerimony. This is the
/'UJal
/piril
of
nitre.
S,iril o/ Wine tombind ,",ilh Ihe Add
.¡
Se. fo/I .
Du/djed Spiril
of
Sall.
M,
x logether, litlle by linle, in a gla(s reton, two
pans of (pirit of wine wilh
on~
pan of (pirit of falt. Set
Ihis miXll1re tOdigefl for a momh in a gende heat, and
diniJl it, tiJl nothin¡¡ remaio io Ihe relon but a thiek
maller.
1'he acia of fea·fall il much lefs
.dif~of~d
10
unite with
s
T
n
Y.
inflammable matters than the other two· mineral :Kid,.
and Ihere(ore, ,houSh il be ever (o highly eonceotraled,
when mixed with (piril of ",ine, il never produces elfer·
vefcence eompmble tO Ihat which is produced by Ihe
fpiril o( nitre . Neilher Ihe prorortion nor f1renglh of
Ihe fpiril of falt, reqllilile to prepm the (wm (piril
0('
falt, are un,nimouOy agreed upon uy aUlhor!. Some
direa equal pms 01 Ihe tWOliquors ; while others pre·
fcribe from IIVO to fou r or fi ve pons of (pirit of w;ne to
one pan of (pirit of (alt. Some u(e only common fpirit
of
(.It;
olhen requiTe Ihe (moking (piril diflilled by
means o( fpiril of vitriol.
L.llIy,
Come order the mix·
lure tO be diflilled, a(ler fome days d:gellion; aod o·
Ihers eontenl them(e1ves wilh "arely digefling it. The
\Vhole derends on Ihe degree of flrenglh IVhich the
(ww
fpirit of fa ll is iatended
10
have. This compoGlion, al
weJl as Ihe (lVeet fpirit of nitre, is erleemed iD medici"e
to be very aperitive and diurelie.
When Ihe mixture of fpirit of fall and (pirit of IVine
is dillilled, there comes oy·:r but one liquar, which ap.
pears homogeneous. T his is Ihe
1'"'''' !piril 0/1011.
The nature o( the marine acid is
001
changed in thi.
combi,nalion: Ihe aeid is ooly weakened .nd rendered
more miId ; bUI in other refpeas it retains its c1waaer·
iflic properties.
Oi/r, or Oily
1II0tl''',
Ihal
are
jo/uhle ill Spiril
.r
IVine, foparated /,om Vet,'ah/tI, and djJ!olved hJ
1n"/nI
of
Ihal M,,,jlruulII. TinOum; Elixirl;
Varnijlm . Arolllaltc jI,.ng 'UJalul.
PUT into a matras the (ubflanees (rom which you in·
tend tO extraét a tinaure. having fi rfl pounded them, or
pulveri(ed them if they are eapable of it. Pour upon
them (pirit o( wine tO the deplh of th ree fi ngers breadth.
Cover the matras witlt a
piec~
of wet bladder, and tie it
00
with packthread. M,ke a little hol. io Ihis bit of
bladder with a pin, leaving il in the Itole to keep it Ilop.
pedo
Set the mams in a (and·bath very gendy hemd.
Iflhe (pirit of wine dilfolve aoy par! of the body. it will
accordingly aequire a deeper or lighter eolour. Con·
tinue the digellioo till. you perceive tbat Ibe fpiril of
wine gains
00
more colour. From time
lO
time pull out
the pin,
10
gi"e vem
10
the vapours,
Of
rarefied air,
which might otherlVi(e burfl the matras. Deeanl your
fpiril of wine, . nd keepit in a bonle weJl eorked. Pour
00
fome frelh (pirit in its rlead : digefl as before ; aod
go on in this manner. pouriog on and off frelh fpirit of
wine, tiJl the lall come off colourle(,.
Spirit of wioe impregnaled wilh (uch par!! of aoy ve–
gelable (ubllance as it is eapable o( dilfolving, is commoo–
Iy ealled a
linfllln.
S~veral
tina ures mixed togelber,
or a tinaure drawn from Cundry vegelable Cubflances at
the Came time, aod in the fame velfc!, take Ibe name of
an
,/ixir.
Tinaures of elixirs impregnated with "fin·
oUs manel! only,are true
varnljl¡,r.
AlI thefe prepara·
,ions are made in the fame
mann~r ;
lowit, as direaed
in our proce(s. We Ihall only add here, Ihal i( Ihe (ub·
flances (rom whieh a tinaure or elixir is
10
be made
contain
100
ml1ch moiflure, it is proper
lO
free Ihero
from it bygentle deGccation; eCpeciallyi(
y~l1
dcGgn Ihat
lhe tioéture lhould
be
weJl impregnated wilb Ihe oilyand
leGoou,